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Thiotrithiazyl Hydrogen Sulphate, N3S4.HSO4

Thiotrithiazyl Hydrogen Sulphate, N3S4.HSO4, is obtained when thiotrithiazyl chloride is dissolved in concentrated sulphuric acid. There is an evolution of hydrogen chloride and, on addition of acetic acid to the solution, the hydrogen sulphate is- deposited as pale yellow needles.

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